Yield, Esterification Degree and Molecular Weight Evaluation of Pectins Isolated from Orange and Grapefruit Peels under Different Conditions
Identifieur interne : 000007 ( Main/Exploration ); précédent : 000006; suivant : 000008Yield, Esterification Degree and Molecular Weight Evaluation of Pectins Isolated from Orange and Grapefruit Peels under Different Conditions
Auteurs : Mohamed Yassine Sayah [Maroc] ; Rachida Chabir [Maroc] ; Hamid Benyahia [Maroc] ; Youssef Rodi Kandri [Maroc] ; Fouad Ouazzani Chahdi [Maroc] ; Hanan Touzani [Maroc] ; Faouzi Errachidi [Maroc]Source :
- PLoS ONE [ 1932-6203 ] ; 2016.
Abstract
Orange (
Url:
DOI: 10.1371/journal.pone.0161751
PubMed: 27644093
PubMed Central: 5028049
Affiliations:
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en">Yield, Esterification Degree and Molecular Weight Evaluation of Pectins Isolated from Orange and Grapefruit Peels under Different Conditions</title><author><name sortKey="Sayah, Mohamed Yassine" sort="Sayah, Mohamed Yassine" uniqKey="Sayah M" first="Mohamed Yassine" last="Sayah">Mohamed Yassine Sayah</name><affiliation wicri:level="1"><nlm:aff id="aff001"><addr-line>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes, Morocco</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes</wicri:regionArea><wicri:noRegion>Fes</wicri:noRegion></affiliation></author><author><name sortKey="Chabir, Rachida" sort="Chabir, Rachida" uniqKey="Chabir R" first="Rachida" last="Chabir">Rachida Chabir</name><affiliation wicri:level="1"><nlm:aff id="aff002"><addr-line>Laboratory of Pathophysiology and Nutrition, Faculty of Medicine and Pharmacy, University Sidi Mohamed Ben Abdelah, Fes, Morocco</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratory of Pathophysiology and Nutrition, Faculty of Medicine and Pharmacy, University Sidi Mohamed Ben Abdelah, Fes</wicri:regionArea><wicri:noRegion>Fes</wicri:noRegion></affiliation></author><author><name sortKey="Benyahia, Hamid" sort="Benyahia, Hamid" uniqKey="Benyahia H" first="Hamid" last="Benyahia">Hamid Benyahia</name><affiliation wicri:level="1"><nlm:aff id="aff003"><addr-line>Laboratoire d'Amélioration et Biotechnologie des Agrumes Institut National de La Recherche Agronomique (INRA) Kenitra, Maroc</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratoire d'Amélioration et Biotechnologie des Agrumes Institut National de La Recherche Agronomique (INRA) Kenitra</wicri:regionArea></affiliation></author><author><name sortKey="Rodi Kandri, Youssef" sort="Rodi Kandri, Youssef" uniqKey="Rodi Kandri Y" first="Youssef" last="Rodi Kandri">Youssef Rodi Kandri</name><affiliation wicri:level="1"><nlm:aff id="aff001"><addr-line>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes, Morocco</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes</wicri:regionArea><wicri:noRegion>Fes</wicri:noRegion></affiliation></author><author><name sortKey="Ouazzani Chahdi, Fouad" sort="Ouazzani Chahdi, Fouad" uniqKey="Ouazzani Chahdi F" first="Fouad" last="Ouazzani Chahdi">Fouad Ouazzani Chahdi</name><affiliation wicri:level="1"><nlm:aff id="aff001"><addr-line>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes, Morocco</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes</wicri:regionArea><wicri:noRegion>Fes</wicri:noRegion></affiliation></author><author><name sortKey="Touzani, Hanan" sort="Touzani, Hanan" uniqKey="Touzani H" first="Hanan" last="Touzani">Hanan Touzani</name><affiliation wicri:level="1"><nlm:aff id="aff001"><addr-line>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes, Morocco</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes</wicri:regionArea><wicri:noRegion>Fes</wicri:noRegion></affiliation></author><author><name sortKey="Errachidi, Faouzi" sort="Errachidi, Faouzi" uniqKey="Errachidi F" first="Faouzi" last="Errachidi">Faouzi Errachidi</name><affiliation wicri:level="1"><nlm:aff id="aff004"><addr-line>Laboratory of Physiology and Molecular Genetics, University Hassan II Ain Chock Faculty of Sciences, Casablanca, Morocco</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratory of Physiology and Molecular Genetics, University Hassan II Ain Chock Faculty of Sciences, Casablanca</wicri:regionArea><wicri:noRegion>Casablanca</wicri:noRegion></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">PMC</idno><idno type="pmid">27644093</idno><idno type="pmc">5028049</idno><idno type="url">http://www.ncbi.nlm.nih.gov/pmc/articles/PMC5028049</idno><idno type="RBID">PMC:5028049</idno><idno type="doi">10.1371/journal.pone.0161751</idno><date when="2016">2016</date><idno type="wicri:Area/Pmc/Corpus">001098</idno><idno type="wicri:Area/Pmc/Curation">001097</idno><idno type="wicri:Area/Pmc/Checkpoint">000003</idno><idno 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Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes, Morocco</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes</wicri:regionArea><wicri:noRegion>Fes</wicri:noRegion></affiliation></author><author><name sortKey="Chabir, Rachida" sort="Chabir, Rachida" uniqKey="Chabir R" first="Rachida" last="Chabir">Rachida Chabir</name><affiliation wicri:level="1"><nlm:aff id="aff002"><addr-line>Laboratory of Pathophysiology and Nutrition, Faculty of Medicine and Pharmacy, University Sidi Mohamed Ben Abdelah, Fes, Morocco</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratory of Pathophysiology and Nutrition, Faculty of Medicine and Pharmacy, University Sidi Mohamed Ben Abdelah, Fes</wicri:regionArea><wicri:noRegion>Fes</wicri:noRegion></affiliation></author><author><name sortKey="Benyahia, Hamid" sort="Benyahia, Hamid" uniqKey="Benyahia H" first="Hamid" last="Benyahia">Hamid Benyahia</name><affiliation wicri:level="1"><nlm:aff id="aff003"><addr-line>Laboratoire d'Amélioration et Biotechnologie des Agrumes Institut National de La Recherche Agronomique (INRA) Kenitra, Maroc</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratoire d'Amélioration et Biotechnologie des Agrumes Institut National de La Recherche Agronomique (INRA) Kenitra</wicri:regionArea></affiliation></author><author><name sortKey="Rodi Kandri, Youssef" sort="Rodi Kandri, Youssef" uniqKey="Rodi Kandri Y" first="Youssef" last="Rodi Kandri">Youssef Rodi Kandri</name><affiliation wicri:level="1"><nlm:aff id="aff001"><addr-line>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes, Morocco</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes</wicri:regionArea><wicri:noRegion>Fes</wicri:noRegion></affiliation></author><author><name sortKey="Ouazzani Chahdi, Fouad" sort="Ouazzani Chahdi, Fouad" uniqKey="Ouazzani Chahdi F" first="Fouad" last="Ouazzani Chahdi">Fouad Ouazzani Chahdi</name><affiliation wicri:level="1"><nlm:aff id="aff001"><addr-line>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes, Morocco</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes</wicri:regionArea><wicri:noRegion>Fes</wicri:noRegion></affiliation></author><author><name sortKey="Touzani, Hanan" sort="Touzani, Hanan" uniqKey="Touzani H" first="Hanan" last="Touzani">Hanan Touzani</name><affiliation wicri:level="1"><nlm:aff id="aff001"><addr-line>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes, Morocco</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratory of Applied Organic Chemistry, University Sidi Mohamed Ben Abdellah, Faculty of Science and Technology, Fes</wicri:regionArea><wicri:noRegion>Fes</wicri:noRegion></affiliation></author><author><name sortKey="Errachidi, Faouzi" sort="Errachidi, Faouzi" uniqKey="Errachidi F" first="Faouzi" last="Errachidi">Faouzi Errachidi</name><affiliation wicri:level="1"><nlm:aff id="aff004"><addr-line>Laboratory of Physiology and Molecular Genetics, University Hassan II Ain Chock Faculty of Sciences, Casablanca, Morocco</addr-line></nlm:aff><country xml:lang="fr">Maroc</country><wicri:regionArea>Laboratory of Physiology and Molecular Genetics, University Hassan II Ain Chock Faculty of Sciences, Casablanca</wicri:regionArea><wicri:noRegion>Casablanca</wicri:noRegion></affiliation></author></analytic><series><title level="j">PLoS ONE</title><idno type="eISSN">1932-6203</idno><imprint><date when="2016">2016</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><p>Orange (<italic>Citrus sinensis</italic>) and grapefruit (<italic>Citrus paradise</italic>) peels were used as a source of pectin, which was extracted under different conditions. The peels are used under two states: fresh and residual (after essential oil extraction). Organic acid (citric acid) and mineral acid (sulfuric acid) were used in the pectin extraction. The aim of this study is the evaluation the effect of extraction conditions on pectin yield, degree of esterification “DE” and on molecular weight “Mw”. Results showed that the pectin yield was higher using the residual peels. Moreover, both peels allow the obtainment of a high methoxyl pectin with DE >50%. The molecular weight was calculated using Mark-Houwink-Sakurada equation which describes its relationship with intrinsic viscosity. This later was determined using four equations; Huggins equation, kramer, Schulz-Blaschke and Martin equation. The molecular weight varied from 1.538 x10<sup>05</sup> to 2.47x10<sup>05</sup> g/mol for grapefruit pectin and from 1.639 x10<sup>05</sup> to 2.471 x10<sup>05</sup> g/mol for orange pectin.</p></div></front><back><div1 type="bibliography"><listBibl><biblStruct><analytic><author><name sortKey="Batisse, C" uniqKey="Batisse C">C Batisse</name></author><author><name sortKey="Fils Lycaon, B" uniqKey="Fils Lycaon B">B Fils-Lycaon</name></author><author><name sortKey="Buret, M" uniqKey="Buret M">M Buret</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Liu, Y" uniqKey="Liu Y">Y Liu</name></author><author><name sortKey="Ahmad, H" uniqKey="Ahmad H">H Ahmad</name></author><author><name sortKey="Luo, Y" uniqKey="Luo Y">Y Luo</name></author><author><name sortKey="Gardiner, Dt" uniqKey="Gardiner D">DT Gardiner</name></author><author><name sortKey="Gunasekera, Rs" uniqKey="Gunasekera R">RS Gunasekera</name></author><author><name sortKey="Mckeehan, Wl" 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